Page 98 - Raw Diet References Book 2019

V Analytical Methods

In order to obtain representative results, samples To obtain a representative analysis, multiple samples
have to be collected and treated according to coming from different batches have to be analysed.
the general principles laid down in Commission A composite sample made from multiple samples is
Regulation (EC) No 152/2009 of 27 January 2009 also valid. To evaluate the results of a single-sample
establishing Community methods of sampling and analysis, maximum tolerances for deviation from the
analysis for the official control of feeding stuffs. declared values, as foreseen in ANNEX 4 of Regulation
767/2009 on the marketing and use of feed should be
The analysis of only one sample may not reflect the permitted as well as tolerances for analytical latitudes.
level declared in the average analysis of the product.

TABLE V-1. NON-EXHAUSTIVE LIST OF ANALYTICAL METHODS

Nutrient Method Reference(S)

Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Sampling
ISO/DIS 6491
Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Moisture
ISO /DIS 6496
Protein (crude) Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Arginine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Histidine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Isoleucine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Lysine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Methionine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Cystin/Cystein Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Phenylalanine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Tyrosine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Threonine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Valine Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Tryptophane
2nd ISO/CD 13904
Fat (crude) Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
VDLUFA method 5.6.2
B.S.I method BS684: section 2.34 :
Linoleic Acid
ISO 5509-1997
AOAC 15th ed. (1990) 969.33 & 963.22

VDLUFA method 5.6.2
B.S.I method BS684: section 2.34 :
Arachidonic Acid
ISO 5509-1997
AOAC 15th ed. (1990) 969.33 & 963.22
Fiber (crude) Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Ash (crude) Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Regulation (EC) 152/2009 O.J. 26/02/2009 L 54
Calcium
ISO/DIS 6869

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